Effect of mechanically activated recycled concrete powder on the properties of cement paste

Szabó Roland; Bárány Tamás Péter; Németh Noémi; Ambrus Mária; Mucsi Gábor

doi:10.5937/ror2501011S

Authors

Szabó Roland University of Miskolc, Institute of Raw Materials Preparation and Environmental Technology, Miskolc, Hungary Author
Bárány Tamás Péter University of Miskolc, Institute of Raw Materials Preparation and Environmental Technology, Miskolc, Hungary Author
Németh Noémi University of Miskolc, Institute of Raw Materials Preparation and Environmental Technology, Miskolc, Hungary Author
Ambrus Mária University of Miskolc, Institute of Raw Materials Preparation and Environmental Technology, Miskolc, Hungary Author
Mucsi Gábor University of Miskolc, Institute of Raw Materials Preparation and Environmental Technology, Miskolc, Hungary Author

DOI:

https://doi.org/10.5937/ror2501011S

Keywords:

recycled concrete powder, compressive strength, mechanical activation, rheology, setting time

Abstract

This study investigates the effect of mechanically activated recycled concrete powder (RCP) on Portland cement mixtures with an RCP content of 20 % is investigated. The setting time tests showed that the inclusion of RCP increased the setting time in almost all cases. However, better results were achieved with the mechanically activated RCP than with the RCP raw material additive. In addition, the final setting time was reduced by almost one hour overall (from 380 min to 325 min) when the 3 minute grind was used, which had a similar setting time to Portland cement. The mixtures showed similar behavior in the rheological tests, with the initial shear stress decreasing slightly after the addition of the RCP. Overall, the compressive strength of the RCP-containing mixtures decreased compared to the cement-containing samples. However, a positive effect of milling was observed, as the lowest compressive strength reduction of 29.34 % was achieved by the RCP ground for 3 minutes.

References

Ahmad K. M., Kristály F., Turzó Z., Effects of clay mineral and physico-chemical variables on sandstone rock permeability, Journal of Oil, Gas and Petrochemical Sciences, 1(1), 2018, 18-26

https://doi.org/10.30881/jogps.00006

Amor F., Diouri A., Ellouzi I., Ouanji F., Development of Zn-Al-Ti mixed oxides-modified cement phases for surface photocatalytic performance, Case Studies in Construction Materials, 9, 2018, e00209

https://doi.org/10.1016/j.cscm.2018.e00209

Cantero B., Bravo M., de Brito J., Sáez del Bosque I. F., Medina C., Mechanical behavior of structural concrete with ground recycled concrete cement and mixed recycled aggregate, Journal of Cleaner Production, 275, 2020, 122913

https://doi.org/10.1016/j.jclepro.2020.122913

Chen X., Li Y., Bai H., Ma L., Utilization of recycled concrete powder in cement composite: strength, microstructure and hydration characteristics, Journal of Renewable Materials, 9 (12), 2021, 2189-2208

https://doi.org/10.32604/jrm.2021.015394

Cho J., Waetzig G. R., Udayakantha M., Hong C. Y., Banerjee S., Incorporation of hydroxyethylcellulose-functionalized halloysite as a means of decreasing the thermal conductivity of oilwell cement, Scientific Reports, 8, 2018, 16149

https://doi.org/10.1038/s41598-018-34283-0

Dacić A., Fenyvesi O., Kopecskó K., Investigation of waste perlite, recycled concrete powders as supplementary cementitious materials, Periodica Polytechnica Civil Engineering, 67 (3), 2023, 683-694

https://doi.org/10.3311/PPci.21593

Deng X., Li J., Lu Z., Zhang J., Luo K., Niu Y., Hu J., He K., Rheological and early hydration of cementitious material containing recycled concrete powders collected from recycled aggregates, Construction and Building Materials, 393, 2023, 132108

https://doi.org/10.1016/j.conbuildmat.2023.132108

dos Reis G. S., Grigore Cazacliu B., Rodriguez Correa C., Ovsyannikova E., Kruse A., Hoffmann Sampaio C., Lima E. C., Dotto G. L., Adsorption and recovery of phosphate from aqueous solution by the construction and demolition wastes sludge and its potential use as phosphate-based fertilizer, Journal of Environmental Chemical Engineering, 8 (1), 2020, 103605

https://doi.org/10.1016/j.jece.2019.103605

Du J., Zhang T., Chen P., Guo Y., Zhan B., Wei J., Yu Q., Phase separation of recycled concrete powder during grinding and consequent influences on its hydration behaviors in cement paste, Cement and Concrete Composites, 142, 2023, 105203

https://doi.org/10.1016/j.cemconcomp.2023.105203

Figueiredo P. O., Ulsen C., Bergerman M. G., Mucsi G., Properties of recycled concrete aggregate produced by different comminution methods, Proceedings of the International V4 Waste Recycling 21 Conference, Miskolc, Hungary, November 2018, 219-227., Editor: Bokányi L., Publisher: University of Miskolc, ISBN 978-963-358-173-5

Gao Q., Li X., Shi X., Li X., Lyu X., Zhu X., Ren Y., Clean and high-value recycling approach for waste concrete powder: Mechano-chemical activation of pozzolanic activity, Powder Technology, 458, 2025, 120988

https://doi.org/10.1016/j.powtec.2025.120988

Greinert A., Piernik A., Grande U., Hulisz P., Construction and demolition waste (CDW) in urban soils as a factor controlling their diversity, Geoderma, 449, 2024, 117019

https://doi.org/10.1016/j.geoderma.2024.117019

Horgnies M., Chen J. J., Bouillon C., Overview about the use of Fourier transform infrared spectroscopy to study cementitious materials, WIT Transactions on Engineering Sciences, WIT Press, 77, 2013, 251-262

https://doi.org/10.2495/MC130221

Ilcan H., Sahin O., Kul A., Ozcelikci E., Sahmaran M., Rheological property and extrudability performance assessment of construction and demolition waste-based geopolymer mortars with varied testing protocols, Cement and Concrete Composites, 136, 2023, 104891

https://doi.org/10.1016/j.cemconcomp.2022.104891

Juhász A. Z., Opoczky L., Mechanical activation of minerals by grinding. Pulverizing and morphology of practices, Budapest: Akadémiai Kiadó - Chichester: Ellis Horwood Ltd Publishers, 1990. ISBN: 0745800157

Kaptan K., Cunha S., Aguiar J., A Review of the Utilization of Recycled Powder from Concrete Waste as a Cement Partial Replacement in Cement-Based Materials: Fundamental Properties and Activation Methods, Applied Sciences, 14 (21), 2024, 9775

https://doi.org/10.3390/app14219775

Khan Z. A., Balunaini U., Costa S., Nguyen N. H.T., A review on sustainable use of recycled construction and demolition waste aggregates in pavement base and subbase layers, Cleaner Materials, 13, 2024, 100266

https://doi.org/10.1016/j.clema.2024.100266

Kong, X., Yao Y., Kai M., Guan Y., Ding X., Gu Z., Liu J., The assessment of the mechanical and durability properties of mortar prepared with carbon dioxide-treated recycled concrete-brick powder, Construction and Building Materials, 466, 2025, 140305

https://doi.org/10.1016/j.conbuildmat.2025.140305

Kumar S., Mucsi G., Kristály F., Pekker P., Mechanical activation of fly ash and its influence on micro and nano-structural behaviour of resulting geopolymers. Advanced Powder Technology, 28 (3), 2017, 805-813

https://doi.org/10.1016/j.apt.2016.11.027

Li Z., Bian Y., Zhao J., Wang Y., Yuan Z., Recycled concrete fine powder (RFP) as cement partial replacement: influences on the physical properties, hydration characteristics, and microstructure of blended cement, Journal of Building Engineering, 62, 2022, 105326

https://doi.org/10.1016/j.jobe.2022.105326

Li J., Zhan B., Gao P., Hu L., Qiao M., Sha H., Yu Q., Effects of recycled concrete powders on the rheology, setting and early age strength of cement paste, Construction and Building Materials, 401, 2023, 132899

https://doi.org/10.1016/j.conbuildmat.2023.132899

Li X., Wang X. Y., Li M., Zhan Q. W., Dong W. Y., Study on activation and performance of recycled hardened concrete powder based on microbial accelerated carbonization, Biochemical Engineering Journal, 214, 2025, 109586

https://doi.org/10.1016/j.bej.2024.109586

Lotfi S., Eggimann M., Wagner E., Mróz R., Deja J., Performance of recycled aggregate concrete based on a new concrete recycling technology, Construction and Building Materials, 95, 2015, 243-256

https://doi.org/10.1016/j.conbuildmat.2015.07.021

Lu B., Shi C. Zhang J. Wang J., Effects of carbonated hardened cement paste powder on hydration and microstructure of Portland cement, Construction and Building Materials, 186, 2018, 699-708

https://doi.org/10.1016/j.conbuildmat.2018.07.159

Luciano A., Cutaia L., Altamura P., Penalvo E., Critical issues hindering a widespread construction and demolition waste (CDW) recycling practice in EU countries and actions to undertake: the stakeholder's perspective, Sustainable Chemistry and Pharmacy, 29, 2022, 100745

https://doi.org/10.1016/j.scp.2022.100745

Menegaki M., Damigos D., Review on current situation and challenges of construction and demolition waste management, Current Opinion in Green and Sustainable Chemistry, 13, 2018, 8-15

https://doi.org/10.1016/j.cogsc.2018.02.010

Methods of testing cement. Part 3: Determination of setting times and soundness, MSZ EN 196-3:2017 Standard, 2017

Mucsi G., Halyag Papné N., Ulsen C., Figueiredo P. O., Kristály F., Mechanical activation of construction and demolition waste in order to improve its pozzolanic reactivity, ACS Sustainable Chemistry & Engineering, 9 (9), 2021, 3416-3427

https://doi.org/10.1021/acssuschemeng.0c05838

Nagataki S., Gokce A., Saeki T., Hisada M., Assessment of recycling process induced damage sensitivity of recycled concrete aggregates, Cement and Concrete Research, 34 (6), 2004, 965-971

https://doi.org/10.1016/j.cemconres.2003.11.008

Németh N., Kristály F., Gál P., Móricz F., Lukács R., Metavolcanic formations in the Paraautochthonous Triassic successions of the Bükk Mts, NE Hungary, International Journal of Earth Sciences (Geol Rundsch) 112, 2023, 297-320

https://doi.org/10.1007/s00531-022-02246-6

Pallewatta S., Weerasooriyagedara M., Bordoloi S., Sarmah A.K., Vithanage M., Reprocessed construction and demolition waste as an adsorbent: an appraisal, Science of The Total Environment, 882, 2023, 163340

https://doi.org/10.1016/j.scitotenv.2023.163340

Pan X., Shi C., Hu X., Ou Z., Effects of CO 2 surface treatment on strength and permeability of one-day-aged cement mortar, Construction and Building Materials, 154, 2017, 1087-1095

https://doi.org/10.1016/j.conbuildmat.2017.07.216

Quan H. Z., Effects of Adhered Mortar Content on Quality of Recycled Coarse Aggregate of Concrete, Advanced Materials Research, 194-196, 2011, 1059-1062

https://doi.org/10.4028/www.scientific.net/AMR.194-196.1059

Santos R. P., Tubino R., Potential evaluation of the use of construction and demolition waste (CDW) in the recovery of degraded soils by mining in Brazil, Resources, Conservation & Recycling Advances, 12, 2021, 200060

https://doi.org/10.1016/j.rcradv.2021.200060

Shen Z., Zhu H., Zhao Z., Pang S., Li Z., Yang S., Cao P., Lin S., High-performance artificial aggregate prepared with recycled concrete powder and its impact on concrete properties, Construction and Building Materials, 404, 2023, 133151

https://doi.org/10.1016/j.conbuildmat.2023.133151

Szabó R., Szűcs M., Ambrus M., Mucsi G., Increasing the pozzolanic reactivity of recovered CDW cement stone by mechanical activation, Materials Proceedings, 13 (1), 2023, 27

https://doi.org/10.3390/materproc2023013027

Tam V.W.Y., Soomro M., Evangelista A.C.J., Quality improvement of recycled concrete aggregate by removal of residual mortar: A comprehensive review of approaches adopted. Construction and Building Materials, 288, 2021, 123066

https://doi.org/10.1016/j.conbuildmat.2021.123066

Tan J., Cai J., Li X., Pan J., Li J., Development of eco-friendly geopolymers with ground mixed recycled aggregates and slag, Journal of Cleaner Production, 256, 2020, 120369

https://doi.org/10.1016/j.jclepro.2020.120369

Tang Q., Ma Z., Wu H., Wang W., The utilization of eco-friendly recycled powder from concrete and brick waste in new concrete: A critical review. Cement Concrete. Composites. 114, 2020, 103807

https://doi.org/10.1016/j.cemconcomp.2020.103807

Tavira J., Jiménez J. R., Ledesma E. F., López-Uceda A., Ayuso J., Real-scale study of a heavy traffic road built with in situ recycled demolition waste, Journal of Cleaner Production, 248, 2020, 119219

https://doi.org/10.1016/j.jclepro.2019.119219

The World Bank Data, Urban population (% of the total population), 2018 revision, https://data.worldbank.org/indicator/SP.URB.TOTL.IN.ZS, date of access 12.08.2024

Trivedi S. S., Das B. B., Barbhuiya S., Performance of construction and demolition waste as recycled aggregates in concrete - review, Proceedings of the Institution of Civil Engineers - Construction Materials, 178 (1), 2025, 20-47

https://doi.org/10.1680/jcoma.23.00030

Wu H., Liang C., Xiao J., Xu J., Ma Z., Early-age behavior and mechanical properties of cement-based materials with various types and fineness of recycled powder, Structural Concrete, 23(2), 2022, 1253-1272

https://doi.org/10.1002/suco.202000834

Xue C., Tian G., Zhang Y., Wang Z., Qiao H., Su L., Study on the effect of particle size on the basic characteristics of RCP and hydration kinetics of slurry, Construction and Building Materials, 470, 2025, 140540

https://doi.org/10.1016/j.conbuildmat.2025.140540

Zhang J., Ding L., Li F., Peng J., Recycled aggregates from construction and demolition wastes as alternative filling materials for highway subgrades in China, Journal of Cleaner Production, 255, 2020, 120223

https://doi.org/10.1016/j.jclepro.2020.120223

Zhang D., Zhang S., Huang B., Yang Q., Li J., Comparison of mechanical, chemical, and thermal activation methods on the utilisation of recycled concrete powder from construction and demolition waste, Journal of Building Engineering, 61, 2022, 105295

https://doi.org/10.1016/j.jobe.2022.105295

Zhang H., Zhang C., He B., Yi S., Tang L., Recycling fine powder collected from construction and demolition wastes as partial alternatives to cement: A comprehensive analysis on effects, mechanism, cost, and CO2 emission. Journal of Building Engineering, 71, 2023, 106507

https://doi.org/10.1016/j.jobe.2023.106507

Zhao Y ., Gao J., Liu C., Chen X., Xu Z., The particle-size effect of waste clay brick powder on its pozzolanic activity and properties of blended cement, Journal of Cleaner Production, 242, 2020, 118521

https://doi.org/10.1016/j.jclepro.2019.118521